Department of Chemistry, College of Science, Yazd University, P. O. Box: 89195-741, Yazd, Iran
10.22036/org.chem.2021.255031.1257
Abstract
This report provides a description of a novel and efficient procedure for the synthesis of substituted 4H-1,3,4-oxadiazines via reaction of various vinyl cyanides and acetohydrazide in H2O under catalyst-free conditions. The remarkable advantages are the simplicity of the experimental procedures, high yields, and avoidance of organic solvents. Products were characterized by melting point, IR, 1H- and 13C-NMR spectra, and elemental analysis. The desired products were obtained in >85% yields.
Mozafari Vanani, S., & Amrollahi, M. A. (2021). Catalyst-free Preparation of 4H-1,3,4-Oxadiazines in H2O. Organic Chemistry Research, 7(1), 54-60. doi: 10.22036/org.chem.2021.255031.1257
MLA
Sedighe Mozafari Vanani; Mohammad Ali Amrollahi. "Catalyst-free Preparation of 4H-1,3,4-Oxadiazines in H2O". Organic Chemistry Research, 7, 1, 2021, 54-60. doi: 10.22036/org.chem.2021.255031.1257
HARVARD
Mozafari Vanani, S., Amrollahi, M. A. (2021). 'Catalyst-free Preparation of 4H-1,3,4-Oxadiazines in H2O', Organic Chemistry Research, 7(1), pp. 54-60. doi: 10.22036/org.chem.2021.255031.1257
VANCOUVER
Mozafari Vanani, S., Amrollahi, M. A. Catalyst-free Preparation of 4H-1,3,4-Oxadiazines in H2O. Organic Chemistry Research, 2021; 7(1): 54-60. doi: 10.22036/org.chem.2021.255031.1257
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